Table 1: Analytical and physical data for [Pd(TAB)(Meth)] and [Pd(en)(Sar)].
Complexes | Complex (empirical formula) | Mwt (g/mol) | Color | M.P. (°C) | Yield (%) | Found (calc.) % | ||
C | H | N | ||||||
[Pd(TAB)(Meth)] | [Pd(C12H11N4)(C5H11NO2S)] | 633.77 | Dark grey | Above 210 | 80% | 44.2 (43.6) | 4.98 (5.01) | 12.9 (12.7) |
[Pd(en)(Sar)] | [Pd(C2N2H8)(C3H7NO2)] | 255 | Dark brown | Above 200 | Up to 85% | 20.8 (20.07) | 3.5 (3.01) | 14.4 (14.05) |
[Pd(TAB)Cl2] | Pd(C12H11N4)Cl2 | 555 | Light grey | Above 180 | Up to 80% | 25.9 (26.2) | 1.99 (1.8) | 10.09 (10.2) |
[Pd(en)Cl2] | Pd(C2H8N2)Cl2 | 237.41 | Light brown | Above 187 | Up to 93% | 10.1 (9.98) | 3.36 (3.2) | 13.4 (13.5) |